Optical / electrical combination of the autoclave reaction product is used for the electrochemical and photochemical composition under high pressure, while, also be applied and other polymer materials research and development in the area of ??the solar cell. Essential equipment is ideal for high temperature and pressure synthesis and catalytic hydrogenation or reaction time. The product can be achieved simultaneously measuring the temperature needed to measure the speed and add or balance inert gas, put down the pressure and ambient pressure experiments under high pressure to achieve online sample pipetting functions under. Technical Highlights: 1, three electrodes while working under high pressure and used interchangeably (patented design), 2, observe the entire course of the reaction can be achieved throughout the shoot, 2, observation window JGS2 high transmittance quartz glass can be achieved under high-pressure reaction Online light reaction, light transmission rate of 95% (windows imported from Japan), 3, pressure free to set the alarm from overpressure vent (patented design) to replace a one-time permanent rupture disc. 4, the machine uses high-pressure explosion-proof design for easy removal and easy installation, long life safety and security (design patents). Application examples: solar cells and the development of new energy sources, photocatalytic reaction and electrochemical fields of scientific research experiments, Fischer-Tropsch reaction, hydrogenation, polymerization, hydrothermal reaction, heterogeneous reactions and supercritical carbon dioxide reaction. Miniature autoclave No.: ZL201003127577.1 high pressure photocatalytic reactor Patent No.: ZL201003127577.2 Model Specifications: Model condition size volume display accuracy WCGF-25ML Φ40 * 60 25ml ± 1 ℃ WCGF-50ML Φ60 * 80 50ml ± 1 ℃ WCGF-100ML Φ80 * 120 100ml ± 1 ℃ WCGF-200ML Φ80 * 140 200ml ± 1 ℃ WCGF-500ML Φ100 * 180 500ml ± 1 ℃ functional configuration and technical parameters are as follows: ● Design Capacity (effective volume): 25ml, 50ml, 100ml, 200ml, 500ml large capacity to be ordered. ● Design Working temperature: room temperature -250 ° C ● three or more electrodes, calomel electrode / bowl piece electrode / reference electrode / multi-electrode than the folder / conductivity electrode ● design working pressure: 10MPa/20MPA/30MPA (optional) ● kettle material: SU316L stainless steel / titanium / Hastelloy, etc. (optional) ● valves and connecting materials: SU316L stainless steel (optional inlet valve parts) ● reactor vessel: the Teflon-lined Looper inside / quartz glass optical window Looper ● Material: Polished JGS2 Japan imported UV quartz (pressure windows) or sapphire crystal ● illumination window diameter: 30mm-60mm (optional) ● heating device with temperature control and uniformity of heat transfer designs. ● With gas into the function. ● with operating temperature, pressure sensors and displays. ● with magnetic stirring. ● with automatic pressure relief protection ● ● Optional outer protective casing can be gas, liquid sample testing optional lighting unit: with PLS-SXE300C/300CUV, or XPS300 or XPS300UV (with TSCS function, long-term guaranteed Light output stability) to use. Optional accessories: UV direct output unit converged optical output unit external lens unit ◆ Working temperature: up to 250 ℃, temperature display accuracy: ± 1 ℃. Contains a set of standard numerical mixing device, titanium / 316L / Hastelloy reactor body set (one of three), the oil bath heating / electric wire heating / ceramic heating set (three) needle two , ball two and a pressure gauge (a digital pressure gauge optional), 1.5 m stainless steel connecting tube, 300mm line pressure sampling tube, 1.5 m gas-phase analysis of the connecting pipe, wrench set. ◆ stirring speed and temperature are Digital Display 0-1500RPM, speed accuracy ± 5RPM, power supply: 220V, 50HZ, stirring power: 25W-100W with models, heating power: 300W-1000W with insulation layer model: the use of environmentally friendly insulation vacuum forming silicate cotton body insulation layer: E-glass fiber insulation factor: Relative humidity ≤ 35% ≥ 500 trillion when working time: 96 hours continuous working single ◆ minimum pressure reading 1pa (optional high-precision digital pressure gauge and digital pressure sensor. ) ◆ American Standard valve fittings as standard interfaces are standard. Demand valve can be connected with a bottle filled with inert gas, an inert protection experiments for reaction, the reaction was achieved without direct contact with the air. Usage: 1: After opening the package and remove the kettle body heater, the kettle into the body after adding material or conductive material into the heater and tighten, open the control box to make contact with the electrode power to ensure the safety clip to (Note: the need do hydrogenation reactions should first inert gas bottle and the gas valve connection kettle body seeking good) Check needle and demand are in the closed state of the valve, for light irradiation reaction while you need to control the light gambled caliber good response kettle translucent caliber can. Access to power 220V, open switch 2: Adjustment clockwise "stirred" knob adjusted according to the rotational speed suitable for the display position of a large capacity such as agitation or stirring the viscous solution may be appropriate to enhance the stirring up the intensity knob 3: temperature Settings: Click the Setup button "▲" key heating, or press the Set key "▼" key desuperheater will quickly set the desired heating temperature such as: 100 ℃, heating said green light, green light off means Stop, microcomputer temperature and heat will increase the temperature set by the temperature difference between the current size determined by ensuring that no temperature overshoot a warming place, and keep the set value and the display value for the heat balance of ± 2.5 ℃ temperature difference under the heating process easily . 4: The self-tuning function: start auto-tuning feature allows different segments or heating power and heating the solution when the number of irregular heating shortest red temperature minimum balance is best, but after changing the heating medium or self-tuning heating conditions should be re- setting. 5: Start the self-tuning: Press the Shift key five seconds, set the window number flashes enter self-tuning state, after three temperature crossed the number stops flashing, which means that self-tuning end, can be used, but self-tuning required in the "?" initial heating use, self-tuning carried halfway uncertain. 6: After the stirrer has a rubber stopper underneath to protect the external thermocouple sockets not rust and corrosion inside with a turn, then unplug the probe is disconnected, the machine stopped working. If this plug with the external thermocouple should unplug the save, the external thermocouple plug into the socket and lock nut, and then the stainless steel probe into the solution for temperature control heating. 7: The electrical burnout protection function, when the thermocouple bad connection, display window 100 on "1" or "hhhh" green light off, stop heating appliances to be checked before use. Note; 1: To ensure the safe use of the ground wire services, please, please do not feed operations or dry air. 2: In order to extend the use of the product, all with a magnetic stirrer fan motor heat dissipation, while pretending to be heated at high temperature heating experiments in particular experiments, the instrument can not just do the heating use, it should be adjusted to rotate the motor or the speed of rotation state (or idle). Motors and appliances to prevent radiation damage by high temperatures. 3: The end of the high temperature heating, turn off the heat switch, wait a few minutes and then turn off stir switch casual warmth. High temperature heating part, work needs careful not to burn. 4: When the new machine for the first time, the use of electric wire heating jacket has white smoke and the smell of smoke color change from white to brown and then white is a normal phenomenon, because oil and other compounds containing glass fibers in the production process should be ventilated place, can be used normally disappears after a few minutes. 5: When the liquid into the jacket benefits, immediately turn off the power, the instrument ventilated place to be dried before use, to avoid the risk of leakage or electrical short circuit occurs. 6: The relative humidity is too large, the induction may be transmitted through the insulation layer, be sure to ground to avoid leakage. And pay attention to ventilation. Relative humidity range of 35% -85% (non-condensing). 7: long instrument in a dry place when not in non-corrosive environment of the saved. 8: If the content due to improvements to this manual for the product or products covered in this manual are different, without notice, please call to manufacturers to obtain detailed material.